Tasuku Kawashima, Ryosuke S.S. Maki, Yoshikazu Suzuki, Preparation and Microstructure of Electrospun BaTiO3 Fibers, ILCPA Volume 62, International Letters of Chemistry, Physics and Astronomy (Volume 62)
https://www.scipress.com/ILCPA.62.5
Abstract:
    Barium titanate (BaTiO<sub>3</sub>: BT) is widely used in various shapes depending on specific applications. Recently, 1-D ferroelectric ceramics are eagerly studied to innovate on new applications. Electrospinning is a versatile method to prepare 1-D nanomaterials. Here, we have prepared BaTiO<sub>3</sub>/poly (vinyl alcohol) (BT/PVA) composite fibers via the electrospinning method. Suspensions of BT/PVA aq. were prepared with weight ratio of BT:PVA:H<sub>2</sub>O = <i>x</i>:0.1:0.9-<i>x</i> (<i>x</i> = 0.2 and 0.3). Dried electrospun BT/PVA fibers were sintered at 900-1000°C for 2 h in air. Morphological change of the 1-D BT fibers before and after sintering was investigated by using scanning electron microscopy (SEM) observation. Distribution of the fiber diameter before and after sintering was characterized; average diameters of the 1-D BT fibers before and after sintering were 720 nm and 640 nm, respectively.
Keywords:
    BaTiO<sub>3</sub>, Electrospinning, Submicron Fibers