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Thermal Analytical Characteristics by TGA-DTA-DSC Analysis of Carica papaya Leaves from Kachchh

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Abstract:

An experimental study on Carica papaya leaves was carried out in Thermo gravimetric analyzer (TGA), Differential Thermal Analyzer (DTA) and Differential Scanning Calorimetric (DSC) analyzer to investigate the effects of reaction atmosphere on thermal chemical characteristics. Experimental results show that In DSC curve, Endothermic peak at 101 °C is attributed to dehydration/Water loss from surface and pores of the powder sample. Step at 215 °C is associated with second order phase transition such as Glass Transition and it should be further confirmed in second heating (During heat- cool- heat cycle). Endothermic peak at 336 °C is associated protease thermal decomposition /Beta Cyclodextrin breakdown. In the TGA Curve, The initial 4 % weight loss is due to water loss from surface/pores of powder sample. Second weight loss between 200-450 °C is associated to degradation of cellulose and hemicellulose.

Info:

Periodical:
International Letters of Natural Sciences (Volume 26)
Pages:
12-20
DOI:
10.18052/www.scipress.com/ILNS.26.12
Citation:
V. R. Ram et al., "Thermal Analytical Characteristics by TGA-DTA-DSC Analysis of Carica papaya Leaves from Kachchh", International Letters of Natural Sciences, Vol. 26, pp. 12-20, 2014
Online since:
Sep 2014
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