The Analysis of Copper-Iron Metallic Mixture by Means of XRD and XRF

Omar, Halo Dalshad

doi:10.18052/www.scipress.com/ILCPA.64.130

ILCPA > Volume 64 > The Analysis of Copper-Iron Metallic Mixture by...

< Back to Volume

The Analysis of Copper-Iron Metallic Mixture by Means of XRD and XRF

Full Text PDF

Abstract:

The objective of the paper has been given on observations based on studies of the three samples of copper-iron (Cu-Fe) alloy have been prepared from 3gm mass of copper of 99.9 % purity powder and adding 1gm weight of iron powder and adding 1.5gm weight of iron powder. A discussion about simple and low cost preparation of Cu-Fe alloy by Mini Mill 2 Panalytical and preparation of the sample was rotating at 10 min and in case of grinding samples at high speed 300 rpm. Herzog press Panalytical used to produce pressed powder Cu-Fe alloy. The characters of Cu-Fe particles are depending on their size, shape and chemical surroundings. X-Ray Diffraction (XRD) (Model: Panalytical Empyrean) study is most important tool used in powder materials science. For studied three samples the value of (111) plane has the highest value compared to other planes. The spectra obtained were analyzed using X-ray fluorescence (XRF) (Model: Rigaku-NEX CG). From the spectra obtained, there were some elements to be present in the sample were Cu-Fe. The intensity of Cu pure is larger than impurity copper samples analysis by XRD and XRF. Also impurity affects the intensity, (2θ) position and shape of the X-ray spectra.

Info:

Periodical:

International Letters of Chemistry, Physics and Astronomy (Volume 64)

Pages:

130-134

DOI:

https://doi.org/10.18052/www.scipress.com/ILCPA.64.130

Citation:

H. D. Omar, "The Analysis of Copper-Iron Metallic Mixture by Means of XRD and XRF", International Letters of Chemistry, Physics and Astronomy, Vol. 64, pp. 130-134, 2016

Online since:

February 2016

Authors:

Halo Dalshad Omar

Keywords:

Copper-Iron Alloy, Crystallite Size, Intensity, XRD Analysis, XRF Analysis

Export:

RIS, BibTeX, Text

Distribution:

Open Access

This work is licensed under a
Creative Commons Attribution 4.0 International License

References:

[1] Halo Dalshad Omar, Surface analysis and roughness parameters of Copper Metallic, International Letters of Chemistry, Physics and Astronomy Vol. 57 (2015) pp.66-71.

[2] A. sinha, powder metallurgy, Ed., Dhanpat Ral&Sons, Delhi, (1987).

[3] I.N. Svinolobova, P. N. Ostrik, and A. N. Kovzik, Properties of iron-copper masteralloypower, Vol. 36, No. 11-12, (1997).

[4] Claudiu Nicolicescu, Daniel Zorila, Victor Nicoara, Marco Actis Grande , Marius Crivenu, Iulian Stefan, Research regarding the influence of copper powders on tensile strength of sintered steels, Advanced Engineering Forum Vol. 13 (2015).

[5] C. Biselli and D. G. Morris: Acta Metall. Mater. 42 (1994) 163–176.

[6] Jean-Claude Crivello, Tohru Nobuki and Toshiro Kuji, Thermal and Magnetic Properties of Mechanically Alloyed fcc Cu-Fe Supersaturated Solid Solutions, Materials, Transactions, Vol. 49, No. 3(2008)pp. 527to531.

[7] Halo Dalshad Omar, To Investigation the Structure and Morphology of Iron Metallic by Difference Techniques, Department of Physics, School of Science, UniversityofKoya, J. Nano. Adv. Mat. 3No. 2, 57-61, (2015).

[8] M. Barzegar Vishlaghi, A. Ataie, Investigation on solid solubility and physical properties of Cu–Fe/CNT nano-composite prepared via mechanical alloying route, Powder Technology 268(2014) 102–109.

[9] Charles Kittel, Introduction to Solid State Physics(ISBN 047141526X) Wiley, 8thEdition, (2004).

[10] N. Habubi, M. Hashim and A. Al-Yasiri, Baghdad Science Journal, 7(2010) 1421.

[11] W. Peng , G. Cong, S. Qu and Z. Wang, Optical Materials , 29 (2006) 313.

[12] F.M. Lucas , B. Trindade , B.F.O. Costa , G. Le Caër, The Influence of PreMilling on the Microstructural Evolution During Mechanical Alloying of a Fe50Cu50 Alloy, Journal of Metastable and Nanocrystalline Materials eVolume 18 (2003)pp.49-56.

[13] H. Wang, X. Lu, Y. Zhao and C. Wang, Materials Letters, 60 (2006) 2480.

[14] D. Awschalom, andJ. Kikkawa, Phys. Today, 52(1999)33.

[15] B. D. Cullity and S. R. Stock, Elements of X-Ray Diffraction, Associate Professor of Metallurgyin, University of Notre Dame, (1978).

[16] Kenji Sakurai and Hiromi Eba, X-Ray Fluorescence Analysis with a Johansson-type Spectrometer, National Research Institute for Metals, 1-2-1, Sengen, Tsukuba, Ibaraki305-0047, Japan, 2 November1998.

Show More Hide

Cited By:

[1] L. Lindawati, M. Mursal, I. Irwansyah, N. Fitriadi, E. Saputra, "Mineral Identification of South Aceh Marble by Using X-Ray Diffraction Method", IOP Conference Series: Materials Science and Engineering, Vol. 536, p. 012005, 2019

DOI: https://doi.org/10.1088/1757-899X/536/1/012005