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International Letters of Chemistry, Physics and Astronomy
Volume 36

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Effect of High-Temperature Heating on Chemical Changes in M7C3 Carbides of AISI D2 Tool Steel

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Abstract:

The paper presents the study results obtained on 16H12MF/NC11LV/D2 tool steel. The main purpose of the study was to establish the chemical composition of the coarse primary M7C3 carbides occurring in that steel after a standard soft annealing. The effect of high-temperature annealing in the air atmosphere was investigated. The study was limited to the decarburized layer, on the distance of about 0.4 mm from the surface, of hardened steel after annealing and austenitizing at 1150 °C in the air atmosphere for the periods of 30 and 90 minutes. It was found that the coarse primary M7C3 carbides of the annealed D2 tool steel differ significantly as to the contents of Cr, Mo, and V, and in the most degree to the contents of chromium and molybdenum. The average concentration of chromium rises successively with the growth of austenitizing time. On the other hand, the concentrations of molybdenum and vanadium are lower after 30 minutes of austenitizing than their concentrations in the similar carbides of the annealed steel. Prolongation of the austenitizing time up to 90 minutes results in the increase of molybdenum and vanadium contents in the coarse carbides. It was found that austenitizing of AISI D2 tool steel at the temperature of 1150 °C in the air atmosphere leads to precipitation of the second phase, brighter in the BSE_Z pictures, in relation to the matrix of carbides, with the amount and magnitude being higher with the annealing time.

Info:

Periodical:
International Letters of Chemistry, Physics and Astronomy (Volume 36)
Pages:
258-271
Citation:
T. Nykiel and T. Hryniewicz, "Effect of High-Temperature Heating on Chemical Changes in M7C3 Carbides of AISI D2 Tool Steel", International Letters of Chemistry, Physics and Astronomy, Vol. 36, pp. 258-271, 2014
Online since:
Jul 2014
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Metals Handbook, 10th Edition, Vol. 1, Properties and Selection: Irons, Steels, and High-Performance Alloys, ASM International, Materials Park, OH 44073, (1990).

M. Blicharski, Wstęp do inżynierii materiałowej. Stal, WNT, Warszawa, (2004).

T. Sato, Y. Honda, Journal of the Iron and Steel Institute of Japan = Tetsu to Hagane, 41 (11) (1955) 1188.

T. Sato, Y. Honda, Journal of the Iron and Steel Institute of Japan = Tetsu to Hagane, 44 (5) (1958) 565.

Z. Głowacki, PhD Thesis, Politechnika Poznańska, Poznań (1956).

Z. Głowacki, The studies over carbides in chromium steels (in Polish). 5th PAN Seminar of Metallurgy Committee, Zakopane 25-27 April 1968, pp.1-17.

W. Kowalski, Prace Instytutu Mechaniki Precyzyjnej (Transactions of IMP) (in Polish), 14(8) (1966) 1.

A.P. Gulajev, J.E. Sanczyk, Zhurn. Techn. Fiz. 22(11) (1952) 1718.

K. Kałuża, PhD Thesis, Politechnika Poznańska, Poznań, (1979).

T. Nykiel, PhD Thesis, Politechnika Poznańska, Poznań, (1982).

T. Hryniewicz, T. Nykiel, Inżynieria Materiałowa 1 (2000) 32-35.

T. Hryniewicz, T. Nykiel, Proc. of the METAL 2001 10th International Metallurgical and Materials Conference, 15-17 May, 2001, Hotel ATOM, Ostrava, Czech Republic; Symposium C: Paper no. 190.

T. Nykiel, T. Hryniewicz, Proc. 6th Intern. Seminar IFHT, Kyongju TEMF Hotel, Kyongju, Korea, October 15-18, 1997, pp.222-229.

T. Nykiel, T. Hryniewicz, Proc. of the 6th Intern. Seminar IFHT, Kyongju TEMF Hotel, 15-18 October, Korea, 1997, pp.238-245.

T. Nykiel, T. Hryniewicz, Proc. of the 11th Congress of the International Federation for Heat Treatment and Surface Engineering, Florence, Italy, 19-21 October, 1998, 116, pp.87-96.

T. Nykiel, T. Hryniewicz, Metallurgical and Materials Transactions A, 31A (2000) 2661-2665.

T. Nykiel, T. Hryniewicz, Proc. of the METAL 2001 10th International Metallurgical and Materials Conference, 15-17 May, 2001, Hotel ATOM, Ostrava, Czech Republic; Symposium C: Paper no. 191.

T. Nykiel, T. Hryniewicz, L. Lemiesiewicz, Mater. II Pomorskiej Konferencji Naukowej Inżynieria Materiałowa 2001, Gdańsk-Sobieszewo, 31. 05-1. 06. 2001, 167173.

T. Nykiel, T. Hryniewicz, Proc. of 11th International Metallurgical & Materials Conference METAL 2002, 20-22 May 2003, Hradec nad Moravici, Czech Republic, Symp. C, (Steel Products Properties).

T. Nykiel, T. Hryniewicz, Proc. of 11th International Metallurgical & Materials Conference METAL 2002, 14-16 May 2002, Hradec nad Moravici, Czech Republic, Symp. C, p.54.

T. Nykiel, T. Hryniewicz, Proc. of 11th International Metallurgical & Materials Conference METAL 2002, 14-16 May 2002, Hradec nad Moravici, Czech Republic, Symp. C, p.56.

T. Nykiel, T. Hryniewicz, Materiały i Technologie, ed. WM Politechniki Gdańskiej, 1(1) (2003) 125-130.

T. Nykiel, T. Hryniewicz, Advances in Materials Science 4(2) (2003) 49-60.

T. Nykiel, T. Hryniewicz, Advances in Materials Science 4(2) (2003) 61-70.

T. Nykiel, T. Hryniewicz, Proc. of 17th International Metallurgical & Materials Conference METAL 2008, 13-15 May 2008, Hradec nad Moravici, Czech Republic, Symp. C, p.24.

T. Nykiel, T. Hryniewicz, Proc. of 18th International Metallurgical & Materials Conference METAL 2009, 19-21 May 2009, Hradec nad Moravici, Czech Republic, Symp. C, p.10.

T. Nykiel, T. Hryniewicz, Proc. of 18th International Metallurgical & Materials Conference METAL 2009, 19-21 May 2009, Hradec nad Moravici, Czech Republic, Symp. C, p.11.

T. Nykiel, T. Hryniewicz, Trans. Indian Inst. Met. 65(1) (2012) 37-48.

T. Nykiel, T. Hryniewicz, Trans. Indian Inst. Met. 65(2) (2012) 219-230.

T. Nykiel, T. Hryniewicz, Journal of Materials Engineering and Performance. 23(6) (2014) 2050-(2054).

E. Haberling, I. Schruff, Thyssen Edelst. Techn. Ber. 13(1) (1987) 64.

D. Grman, N. Klantschi, C. Solenthaler, Material und Technik 4 (1988) 81.

Z. Bojarski, Prace Instytutu Hutnictwa (in Polish), 12 (1960) 262.

Z. Głowacki, H. Leda, Zeszyty Naukowe Politechniki Poznańskiej (Transactions of PP) (in Polish), 5(37) (1966) 181.

Z. Głowacki, A. Barbacki, Zeszyty Naukowe Politechniki Poznańskiej (Transactions of PP) (in Polish), 6(33) (1965) 133.

J.L. Pouchou, F. Pichoir, La Recherches Aerospatiale, 5 (1984) 13.

T.M. Breunig, F.J. Worzala, Dynamic fracture toughness characteristics of D2 tool steel, Proc. of the 6th Intl. Congress on Heat Treatment and Surface Engineering, Chicago, 28-30 Sept. 1988, pp.207-211.

S.D. Carpenter, D. Carpenter, Materials Letters 57 (2003) 4456.

S.D. Carpenter, D. Carpenter, Materials Letters 57 (2003) 4460.

S.D. Carpenter, D. Carpenter, J.T.H. Pearce, J. Alloys and Compounds 494 (2010) 245.

F. Ernst, D. Li, H. Kahn, G.M. Michal, A.H. Heuer, Acta Materialia 59 (2011) 2268.

M.J. Monteiro, F.C. Rizzo, Mater. Sci. Forum 522-523 (2005) 171.

M. Palcut, V. Vach, R. Cicka, J. Janovec, Archives of Metallurgy and Materials, 53(4) (2008) 1157.

Y. Zhang, G. Zong, K. Shui, M. He, Heat Treatment of Metals 10 (2010) 44.

P. Bała, Archives of Metallurgy and Materials 54(2) (2009) 491.

Molinari, M. Pellizzari, A. Biggi, G. Corbo, A. Tremea, Proc. 6th Intern. Tooling Conference, 2002, [Karlstad University, 10-13 September 2002]. Vol. 2, ed. Jens Bergström, 33_437_452_pdf_66272.

A.K. Sinha, Physical metallurgy handbook, The McGraw-Hill Companies, Inc., (2003).

L. Zhou, D. Sun, C. -S. Liu, Q. Wu, J. Iron and Steel Research Intern. 13(6) (2006) 4952.

F. Ernst, D. Li, H. Kahn, G.M. Michal, A.H. Heuer, Acta Materialia 59 (2011) 22682276.

J. Ryś, Wstęp do metalografii ilościowej (Introduction to quantitative metallurgy; in Polish), ed. by Biblioteka Fizyki Metali, Wydawnictwo Śląsk, Katowice (1970).

K. Sikorski, Przegląd metod korekcji w ilościowej mikroanalizie rentgenowskiej próbek litych (Review of corrections methods in X-ray quantitative analysis of solid samples), in Podstawy ilościowej mikroanalizy rentgenowskiej (in Polish), ed. by A. Szummer, WNT, Warszawa, 1994, pp.140-166.

Thermo-Calc Software TCFE7 Steels/Fe-alloys database version 7, http: /www. thermocalc. com, 2012, http: /web. access. rwth- aachen. de/THERMOCALC/proceedings/proceedings2012/2012_Henrik_Larsson. pdf ( Received 25 June 2014; accepted 04 July 2014 ).

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